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5-(4-Chlorophenyl)-2-methyl-3-furaldehyde → [5-(4-Chlorophenyl)-2-methyl-3-furyl](cyclohexyl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-(4-Chlorophenyl)-2-methyl-3-furaldehyde | HCID 21986471 | — |
| 反応物 | HCID 178420632 | HCID 178420632 | — |
| 生成物 | [5-(4-Chlorophenyl)-2-methyl-3-furyl](cyclohexyl)methanol | HCID 68509840 | 83% |
反応手順
An operation similar to that in Example 3 (2) was performed using 5-(4-chlorophenyl)-2-methyl-3-furaldehyde (1.7 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (15 mL) to give the title compound (2.0 g, 83%) as a white crystal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08309580B2 |
| 出典データセット | uspto-grants-2012_11 |
| ORD ID | ord-922c2f337ed144208328425921ca39fd |
| 出典メモ | uspto-grants-2012_11 |