化工社化工社 化学情報印刷レポート · 研究参考用
5-(4-Fluorophenyl)-2-methyl-3-furaldehyde → Cyclohexyl[5-(4-fluorophenyl)-2-methyl-3-furyl]methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-(4-Fluorophenyl)-2-methyl-3-furaldehyde | HCID 23074370 | — |
| 反応物 | HCID 178420632 | HCID 178420632 | — |
| 生成物 | Cyclohexyl[5-(4-fluorophenyl)-2-methyl-3-furyl]methanol | HCID 68514205 | 83% |
反応手順
An operation similar to that in Example 3 (2) was performed using 5-(4-fluorophenyl)-2-methyl-3-furaldehyde (2.0 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (15 mL) to give the title compound (2.4 g, 83%) as a white crystal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08309580B2 |
| 出典データセット | uspto-grants-2012_11 |
| ORD ID | ord-fa1924eb2a5f4bdaa792e31137d0b159 |
| 出典メモ | uspto-grants-2012_11 |