化工社化工社 化学情報印刷レポート · 研究参考用
(2,4-Dichlorophenyl)boronic acid → Methyl 5-(2,4-dichlorophenyl)-2-methyl-3-furoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (2,4-Dichlorophenyl)boronic acid | HCID 2734659 | — |
| 反応物 | Methyl 5-bromo-2-methylfuran-3-carboxylate | HCID 15534190 | — |
| 生成物 | Methyl 5-(2,4-dichlorophenyl)-2-methyl-3-furoate | HCID 68514435 | 54% |
反応手順
An operation similar to that in Example 49 (2) was performed using methyl 5-bromo-2-methyl-3-furoate (3.3 g) and 2,4-dichlorophenylboronic acid (3.4 g) to give the title compound (2.3 g, 54%) as a yellow crystal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08309580B2 |
| 出典データセット | uspto-grants-2012_11 |
| ORD ID | ord-45891623dc0f40a39a4f542f3e57787f |
| 出典メモ | uspto-grants-2012_11 |