化工社化工社 化学情報印刷レポート · 研究参考用
5-(2,4-Dichlorophenyl)-2-methyl-3-furaldehyde → Cyclohexyl[5-(2,4-dichlorophenyl)-2-methyl-3-furyl]methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-(2,4-Dichlorophenyl)-2-methyl-3-furaldehyde | HCID 83595757 | — |
| 反応物 | HCID 178420632 | HCID 178420632 | — |
| 生成物 | Cyclohexyl[5-(2,4-dichlorophenyl)-2-methyl-3-furyl]methanol | HCID 68511587 | 77% |
反応手順
An operation similar to that in Example 3 (2) was performed using 5-(2,4-dichlorophenyl)-2-methyl-3-furaldehyde (1.3 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (7.5 mL) to give the title compound (1.3 g, 77%) as a white crystal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08309580B2 |
| 出典データセット | uspto-grants-2012_11 |
| ORD ID | ord-85cadfcc69ef4610a00e4d6ba7420bfb |
| 出典メモ | uspto-grants-2012_11 |