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5-(4-Chloro-2-methylphenyl)-2-methyl-3-furaldehyde → [5-(4-Chloro-2-methylphenyl)-2-methyl-3-furyl] (cyclohexyl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-(4-Chloro-2-methylphenyl)-2-methyl-3-furaldehyde | HCID 86646368 | — |
| 溶媒 | HCID 178420632 | HCID 178420632 | — |
| 生成物 | [5-(4-Chloro-2-methylphenyl)-2-methyl-3-furyl] (cyclohexyl)methanol | HCID 68514219 | 156.4% |
反応手順
An operation similar to that in Example 3 (2) was performed using 5-(4-chloro-2-methylphenyl)-2-methyl-3-furaldehyde (1.6 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (10 mL) to give the title compound (1.7 g, 77%) as a white crystal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08309580B2 |
| 出典データセット | uspto-grants-2012_11 |
| ORD ID | ord-190b2a545df64902b5ffe700b3d0a12f |
| 出典メモ | uspto-grants-2012_11 |