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1-(3,4,5-Trimethoxyphenyl)piperazine → 1-[(3,6-Dimethoxyquinoxalin-2-yl)aminocarbonyl]-4-(3,4,5-trimethoxyphenyl)piperazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(3,4,5-Trimethoxyphenyl)piperazine | HCID 3838765 | — |
| 反応物 | ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate | HCID 69244324 | — |
| 生成物 | 1-[(3,6-Dimethoxyquinoxalin-2-yl)aminocarbonyl]-4-(3,4,5-trimethoxyphenyl)piperazine | HCID 69245206 | 92% |
反応手順
Ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate and 1-(3,4,5-trimethoxyphenyl)piperazine were reacted by the same way with the example 148 to obtain the titled compound (yield, 92%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08314100B2 |
| 出典データセット | uspto-grants-2012_11 |
| ORD ID | ord-132163e09aac4d5898a601fec6ff5be5 |
| 出典メモ | uspto-grants-2012_11 |