Dimethylformamide → HCID 67094308、化合物
反応式
[CH2:1]([O:3][C:4]1[C:11]([O:12][CH2:13][CH3:14])=[CH:10][C:7]([CH:8]=O)=[C:6]([N+]([O-])=O)[C:5]=1[N+:18]([O-:20])=[O:19])[CH3:2].[CH3:21]N(C)C=O.C[CH:27]([SH:31])[C:28]([O-:30])=[O:29]>C(N(CC)CC)C>[CH3:21][O:30][C:28]([C:27]1[S:31][C:6]2[C:5]([N+:18]([O-:20])=[O:19])=[C:4]([O:3][CH2:1][CH3:2])[C:11]([O:12][CH2:13][CH3:14])=[CH:10][C:7]=2[CH:8]=1)=[O:29]参加物
5
実験手順
4,5-Diethoxy-2,3-dinitro-benzaldehyde (1.53 g) was dissolved into N,N-dimethylformamide (6 ml) and then methylthioglycolate (1.36 ml) was added. Triethylamine (2.6 ml) was added in cold to the reaction solution. The mixture was stirred overnight. The solid was filtered and washed with N,N-dimethylformamide.
後処理
- filtrationThe solid was filtered
- washwashed with N,N-dimethylformamide
出典と根拠
- ORDレコード
- ord-091b2d51415b43bf900a177f8eefff47
- 出典データセット
- uspto-grants-2012_11
- 特許番号
- US08318785B2
反応ノート
読み込み中…