化工社化工社 化学情報印刷レポート · 研究参考用
2-Hydroxy-11-cycloeicosenone → 2-Hydroxycyclooctadecanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Hydroxy-11-cycloeicosenone | HCID 67312852 | — |
| 反応物 | 2-Hydroxy-9-cyclooctadecenone | HCID 69649678 | — |
| 生成物 | 2-Hydroxycyclooctadecanone | HCID 9878887 | — |
反応手順
2-Hydroxy-11-cycloeicosenone of Synthesis Example 7 was replaced by 2-hydroxy-9-cyclooctadecenone (1.0 g, 3.54 mmol), and a hydrogenation and subsequent treatment were performed under the same conditions as in Synthesis Example 7, to yield 1.0 g of 2-hydroxycyclooctadecanone (quantitative yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06759557B2 |
| 出典データセット | uspto-grants-2004_07 |
| ORD ID | ord-b77a471df5e74655ac77e43502bce19d |
| 出典メモ | uspto-grants-2004_07 |