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HRID 1884674作成日：2026年10月27日

8-Phenyloctan-1-amine → N-(8-phenyl-octyl)-3,5-bis(m-trifluoromethylphenyl)-4-(2-hydroxyethoxy)benzamide

https://huagongshe.com/reaction/1884674

反応式

関与物質

役割名称HCID仕込み量
反応物8-Phenyloctan-1-amineHCID 145556—
反応物3,5-Bis(m-trifluoromethylphenyl)-4-(2-hydroxyethoxy)benzoic acid ethyl esterHCID 54098193—
生成物N-(8-phenyl-octyl)-3,5-bis(m-trifluoromethylphenyl)-4-(2-hydroxyethoxy)benzamideHCID 22237402—

反応手順

N-(8-phenyl-octyl)-3,5-bis(m-trifluoromethylphenyl)-4-(2-hydroxyethoxy)-benzamide was prepared as a white solid (0.331 g, 74%) from 3,5-bis-(m-trifluoromethylphenyl)-4-(2-hydroxyethoxy)benzoic acid ethyl ester and phenyloctyl amine using a procedure similar to step 2 of Example 1. 1H NMR (CDCl3) δ 7.96-7.50 (m, 10H); 7.35-7.10 (m, 5H); 6.28 (m, 1H); 3.45 (m, 2H); 3.31 (m, 4H); 2.60 (m, 2H); 1.60 (m, 4H); 1.33 (m, 8H).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06765021B2
出典データセットuspto-grants-2004_07
ORD IDord-626989193ff0427c9223950da0da6eb2
出典メモuspto-grants-2004_07