化工社化工社 化学情報印刷レポート · 研究参考用
6-Fluoropyridine-2-carboxylic acid → 4-Methylpyridine-2-carbohydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Fluoropyridine-2-carboxylic acid | HCID 226027 | — |
| 反応物 | 6-Fluoropyridine-2-carbohydrazide | HCID 345818 | — |
| 反応物 | 4-Methylpyridine-2-carboxylic acid | HCID 2762820 | — |
| 生成物 | 4-Methylpyridine-2-carbohydrazide | HCID 45084313 | — |
反応手順
4-Methyl-2-pyridinecarbohydrazide was prepared in a manner analogous to that described above for 6-fluoro-2-pyridinecarbohydrazide (I23) but using 4-methyl-2-pyridinecarboxylic acid (CAS [4021-08-3], commercially available e.g. from Sigma-Aldrich or Fluorochem) in the place of 6-fluoro-2-pyridinecarboxylic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08501946B2 |
| 出典データセット | uspto-grants-2013_08 |
| ORD ID | ord-fd9131c7394245519127e020d60965d9 |
| 出典メモ | uspto-grants-2013_08 |