Ammonium Hydroxide → 9-Aminononanoic acid

HRID 1889150

反応式

HRID 1889150 の反応式
Br[CH:2](C)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11].[OH-].[NH4+:15]>>[NH2:15][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11]

参加物

3

反応物 2

HCID 14923Ammonium HydroxideHCID 4684996HCID 4684996、化合物

生成物 1

HCID 1368779-Aminononanoic acid

実験手順

9-bromodecanoic acid (2.0052 gr, 8.46 mmol) was added to a round bottom flask containing 80 mL of aqueous ammonium hydroxide (25% NH3). The resulting mixture was stirred for 24 hours at room temperature, after which the aqueous solution was evaporated under reduced pressure, resulting in product 8a as a white solid at quantitative yield. 1H-NMR (200 MHz, CD3OD): 1.25-1.4 (m; 8H), 1.5-1.7 (m; 4H), 2.23 (t; J=7.31 Hz; 2H), 2.87 (t; J=7.45 Hz; 2H).

後処理

  1. customafter which the aqueous solution was evaporated under reduced pressure

出典と根拠

ORDレコード
ord-fea56029035e4fc1b7b74a0469a11682
出典データセット
uspto-grants-2013_08
特許番号
US08501969B2

関連ノート

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