(1H-Thieno[3,2-c]pyrazol-5-yl)methanol → (1H-Thieno[3,2-c]pyrazol-5-yl)methanaminium chloride

反応式

[NH:1]1[C:5]2[CH:6]=[C:7]([CH2:9]O)[S:8][C:4]=2[CH:3]=[N:2]1.[ClH:11].S1C2C=C[N:17]=CC=2C=C1CN>>[Cl-:11].[NH:1]1[C:5]2[CH:6]=[C:7]([CH2:9][NH3+:17])[S:8][C:4]=2[CH:3]=[N:2]1

参加物

反応物 2

HCID 57354336(1H-Thieno[3,2-c]pyrazol-5-yl)methanol

HCID 67306703Thieno[3,2-c]pyridin-2-ylmethanamine hydrochloride

生成物 1

HCID 86671432(1H-Thieno[3,2-c]pyrazol-5-yl)methanaminium chloride

実験手順

Intermediate F was prepared from (1H-thieno[3,2-c]pyrazol-5-yl)methanol (F-6) following similar procedures for synthesizing intermediate D from D-3, as described above.

出典と根拠

ORDレコード: ord-f401d5b9f9254df9a05d4faad24d9ce9
出典データセット: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08507487B2

反応ノート

読み込み中…