Cyclopropanol → Cyclopropylsulfamate
反応式
[C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH:6]=[CH:5]C=CC=1.[CH:12]1(O)[CH2:14][CH2:13]1>>[CH:12]1([NH:9][S:8](=[O:11])(=[O:10])[O-:7])[CH2:14][CH2:13]1.[CH:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH2:5][CH2:6]1参加物
4
実験手順
Cyclopropylsulfamate was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing cyclopropanol (synthesized by methods reported in JOC 1980, 45, 4129-35) to obtain sulfamic acid cyclopropyl ester.
出典と根拠
- ORDレコード
- ord-f0dba5a8226f48ceb0536a19d496f4b1
- 出典データセット
- uspto-grants-2013_08
- 特許番号
- US08513186B2
反応ノート
読み込み中…