化工社化工社 化学情報印刷レポート · 研究参考用
Thiophosgene → 2-Chloro-4-methylphenyl isothiocyanate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thiophosgene | HCID 10040 | — |
| 反応物 | 2-Chloro-p-toluidine | HCID 12007 | — |
| 反応物 | Diisopropylethylamine | HCID 81531 | — |
| 生成物 | 2-Chloro-4-methylphenyl isothiocyanate | HCID 143529 | 58.3% |
反応手順
The title compound was prepared following the procedure described for intermediate-2 using 2-chloro-4-methyl aniline (2.0 g, 14.00 mmol), thiophosgene (1.62 g, 14.00 mmol) and N-ethyl di-isopropyl amine (3.63 g, 28.00 mmol) to afford 1.5 g of the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08519149B2 |
| 出典データセット | uspto-grants-2013_08 |
| ORD ID | ord-3b59b75f740b42dfa65e357b2132c9af |
| 出典メモ | uspto-grants-2013_08 |