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N-Methylheptylamine → 1-(4-Fluoro-2-nitrophenyl)-3-heptyl-3-methylurea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Methylheptylamine | HCID 93190 | — |
| 反応物 | Phenyl 4-fluoro-2-nitrophenylcarbamate | HCID 23370075 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | 1-(4-Fluoro-2-nitrophenyl)-3-heptyl-3-methylurea | HCID 23370111 | — |
反応手順
Phenyl 4-fluoro-2-nitrophenylcarbamate (0.70 g) and N-methylheptylamine (0.33 g) were dissolved in xylene (5 ml) and the solution was heated under reflux for 2 hrs. The solvent was distilled off and the residue was purified by a silica gel column chromatography (hexane:ethyl acetate=3:1) to give 1-(4-fluoro-2-nitrophenyl)-3-heptyl-3-methylurea as an oily product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05576335 |
| 出典データセット | uspto-grants-1996_11 |
| ORD ID | ord-0ed557f86cb647dda8e553acb0bf24a6 |
| 出典メモ | uspto-grants-1996_11 |