Methylhydrazine → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

HRID 1902139ノート

反応式

HRID 1902139 の反応式

Cl[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3].[CH3:17][NH:18][NH2:19]>CO>[CH3:17][NH:18][NH:19][C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3]

参加物

4

反応物 2

HCID 6061Methylhydrazine

HCID 540353651-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Cloroformate

生成物 1

HCID 544690901-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

The title compound is prepared by reacting the compound of Example 27 (1 mole) with methylhydrazine (1.1 mole) in methanol.

出典と根拠

ORDレコード: ord-b50d9ee2a7eb4b859e89f04fdbfd22bb
出典データセット: uspto-grants-1996_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05578731

反応ノート

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