Hydrochloric Acid → Hydroxylauric Acid

HRID 1902398

反応式

HRID 1902398 の反応式
Cl[CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C:3]([OH:5])=[O:4].[OH-:16].[K+].Cl>O>[OH:16][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C:3]([OH:5])=[O:4]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 14797Potassium HydroxideHCID 43873702-chlorododecanoic Acid

生成物 1

HCID 97783Hydroxylauric Acid

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

0.1 Mole of alpha-chlorolauric acid prepared in the foregoing manner was admixed with 500 mls. water and 0.4 moles of KOH in a suitable reaction vessel and stirred overnight at a temperature of 98°-100° C. The reaction mixture was poured into a separatory funnel, to which was added hydrochloric acid (40 ml. conc. HCl in 200 ml. H2O). The mixture was extracted with chloroform. The chloroform layer was removed and the CHCl3 evaporated to yield alpha-hydroxylauric acid.

後処理

  1. additionThe reaction mixture was poured into a separatory funnel, to which
  2. extractionThe mixture was extracted with chloroform
  3. customThe chloroform layer was removed
  4. customthe CHCl3 evaporated

出典と根拠

ORDレコード
ord-9737ada584704b44899546ddc2bdd5e1
出典データセット
uspto-grants-1982_12
特許番号
US04363763

関連ノート

読み込み中…