Water → Aluminum Chloride Hydrate Thiourea

HRID 1902817

反応式

HRID 1902817 の反応式
[OH2:1].O.O.O.O.O.[Cl-:7].[Al+3:8].[Cl-].[Cl-].[NH2:11][C:12]([NH2:14])=[S:13].O>>[OH2:1].[Cl-:7].[Al+3:8].[Cl-:7].[Cl-:7].[NH2:11][C:12]([NH2:14])=[S:13]

参加物

4

反応物 3

HCID 962WaterHCID 2723790ThioureaHCID 9794789AlCl3.6H2O

生成物 1

HCID 86738713Aluminum Chloride Hydrate Thiourea

反応条件

温度
72 °C

実験手順

In a 5 liter flask is placed 482.8 g. (2.0 mole) aluminum chloride hexahydrate and 1826.8 g. (24.0 moles) thiourea and shaken to mix. To this is added 2284 g. (127 moles) water and heated with stirring to 72° C. to obtain a clear, colorless solution. White crystals form upon cooling leaving a clear solution of pH 1.7 and a final weight of 4592 g.

後処理

  1. customIn a 5 liter flask is placed
  2. additionto mix
  3. additionTo this is added 2284 g
  4. customto obtain a clear, colorless solution
  5. customWhite crystals form
  6. temperatureupon cooling
  7. customleaving a clear solution of pH 1.7

出典と根拠

ORDレコード
ord-92eb2987676b43159ef2fe9e790f12cd
出典データセット
uspto-grants-1982_12
特許番号
US04366096

関連ノート

読み込み中…