反応式
[SH2]=N.[CH2:3]([NH:5][C:6](C1C=CC=CC=1C(O)=O)=[O:7])[CH3:4].[NH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.C(N(CC)CC)C.O>CC(C)=O>[C:18]1([NH:17][C:6]([NH:5][CH2:3][CH3:4])=[O:7])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1参加物
6
実験手順
5.08 g ethylcarbamoyl-benzoic acid sulfimide was reacted with 1.86 g aniline and 2.8 ml triethylamine in 20 ml of a 1:1 mixture of water and acetone, as described in example 1. 2.59 g 1-phenyl-3-ethylurea was obtained, melting at 99°-100° C.
出典と根拠
- ORDレコード
- ord-35440c9b9e2543be8db34146e9f698d2
- 出典データセット
- uspto-grants-1984_03
- 特許番号
- US04435567
関連ノート
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