N-Allyl-2,2'-iminodiethanol → N-[2-(2-Methoxyethoxy)ethyl]diethanolamine
反応式
[CH2:1]([N:4]([CH2:8][CH2:9][OH:10])[CH2:5][CH2:6][OH:7])[CH:2]=C.S(C1C=CC(C)=CC=1)([O:14][CH2:15][CH2:16][O:17][CH2:18]COC)(=O)=O>>[CH3:18][O:17][CH2:16][CH2:15][O:14][CH2:2][CH2:1][N:4]([CH2:8][CH2:9][OH:10])[CH2:5][CH2:6][OH:7]参加物
3
実験手順
The title compound was prepared as described above for N-allyldiethanolamine in Example 1 except that 2-methoxyethoxyethyl tosylate was used (0.55 mol, 150.9 g) in a 0.5 mol preparation. The pure diol whose formula is shown below was obtained (49.8 g, 48%) on fractional distillation at 129°-131° C. (0.04 mm):
後処理
- customin a 0.5 mol preparation
- custombelow was obtained (49.8 g, 48%)
- distillationon fractional distillation at 129°-131° C. (0.04 mm)
出典と根拠
- ORDレコード
- ord-00593ba9d30d4b0892dcb3dd130175ef
- 出典データセット
- uspto-grants-1984_03
- 特許番号
- US04436664
反応ノート
読み込み中…