HCID 54049138、化合物 → HCID 13316973、化合物
反応式
[Br:1][CH2:2][CH2:3][CH:4]=[CH:5][CH2:6][CH2:7][C:8]1[CH:15]=[CH:14][C:11]([C:12]#[N:13])=[CH:10][CH:9]=1>C(O)C.[Pt]=O>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:15]=[CH:14][C:11]([C:12]#[N:13])=[CH:10][CH:9]=1参加物
4
実験手順
A solution of 10.5 g of 4-(6-bromohex-3-enyl)benzonitrile in 200 ml of absolute ethanol was hydrogenated in the presence of 0.25 g of platinum oxide catalyst. Isolation of the product afforded 10.4 g of 4-(6-bromohexyl)benzonitrile as a yellow oil which was distilled at 168°-170° C.(0.01 mm) to produce the compound as a colorless oil which solidfied upon cooling.
出典と根拠
- ORDレコード
- ord-650cfc9ff51a4789b5f4463826c00b89
- 出典データセット
- uspto-grants-1989_06
- 特許番号
- US04843087
反応ノート
読み込み中…