Chloroacetic Acid → 2-[2-(4-Fluorophenyl)ethoxy]acetic acid
反応式
[F:1][C:2]1[CH:10]=[CH:9][C:5]([CH2:6][CH2:7][OH:8])=[CH:4][CH:3]=1.Cl[CH2:12][C:13]([OH:15])=[O:14].CC1CCCCC1>>[F:1][C:2]1[CH:10]=[CH:9][C:5]([CH2:6][CH2:7][O:8][CH2:12][C:13]([OH:15])=[O:14])=[CH:4][CH:3]=1参加物
4
実験手順
7.0 g of 4-fluorophenethyl alcohol were reacted with 4.73 g of chloroacetic acid in a manner analogous to that described in Example 1(a) to give 7.8 g (79%) of 2-(4-fluorophenyl)ethoxyacetic acid of melting point 82°-85° C. (from methylcyclohexane).
出典と根拠
- ORDレコード
- ord-391d245eecff439ab3cf621b91567243
- 出典データセット
- uspto-grants-1987_03
- 特許番号
- US04649160
反応ノート
読み込み中…