2-[2-(4-Fluorophenyl)ethoxy]acetic acid → HCID 13208930、化合物
反応式
[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][O:10][CH2:11][C:12](O)=[O:13])=[CH:4][CH:3]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[F:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][CH2:9][O:10][CH2:11][CH2:12][OH:13])=[CH:6][CH:7]=1参加物
3
実験手順
The 2-(4-fluorophenyl)ethoxyacetic acid obtained according to the preceding paragraph was reduced with lithium aluminum hydride in a manner analogous to that described in Example 1(b) to give 6.6 g (91%) of 2-[2-(4-fluorophenyl)-ethoxy]ethanol in the form of an oil which was homogeneous according to chromatography.
出典と根拠
- ORDレコード
- ord-ba23e3c405ba46ee8fafc1a972d869d4
- 出典データセット
- uspto-grants-1987_03
- 特許番号
- US04649160
反応ノート
読み込み中…