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1,2-Epoxyhexadecane → 3-(2-Hydroxyhexadecyloxy)-2-methoxypropyl tetrahydropyranyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Epoxyhexadecane | HCID 23741 | — |
| 反応物 | HCID 13563077 | HCID 13563077 | — |
| 生成物 | 3-(2-Hydroxyhexadecyloxy)-2-methoxypropyl tetrahydropyranyl ether | HCID 20213822 | 53.2% |
反応手順
The epoxide (9) (4.8 g, 20 mmoles) as obtained in Example 4-1 was reacted with 7.6 g (40 mmoles) of 2-methylglycerol monotetrahydropyranyl ether in the same manner as Example 1-2 to give 4.58 g (53.2%) of the desired compound (10).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04649203 |
| 出典データセット | uspto-grants-1987_03 |
| ORD ID | ord-5d5a4e6881d74511a5e0214a95db749f |
| 出典メモ | uspto-grants-1987_03 |