Hydrochloric Acid → 4-Amino-3-hydroxy-6-methyl-1-phenylheptane hydrochloride

HRID 1906363ノート

反応式

HRID 1906363 の反応式
C(OC([NH:8][CH:9]([CH2:20][CH:21]([CH3:23])[CH3:22])[CH:10]([OH:19])[CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=O)(C)(C)C.[ClH:24]>CO>[ClH:24].[NH2:8][CH:9]([CH2:20][CH:21]([CH3:23])[CH3:22])[CH:10]([OH:19])[CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 138931534-t-Butyloxycarbonylamino-3-hydroxy-6-methyl-1-phenylheptane

生成物 1

HCID 200441484-Amino-3-hydroxy-6-methyl-1-phenylheptane hydrochloride

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

The resultant compound of Example 1 (87 mg, 0.27 mmol) was dissolved in methanol (1 ml) and was treated with methanolic HCl (5 ml of 0.75M). After 15 hours the solution was evaporated to provide the desired compound as a glass (71 mg) which was used without further purification.

後処理

  1. customAfter 15 hours the solution was evaporated

出典と根拠

ORDレコード
ord-906dd61b2f37435788b58d762f0e206a
出典データセット
uspto-grants-1987_03
特許番号
US04652551

反応ノート

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