化工社化工社 化学情報印刷レポート · 研究参考用
Dabco → Diethylaminoethyl 2-(1-hydroxycarbethoxymethyl)-acrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dabco | HCID 9237 | — |
| 反応物 | 2-(Diethylamino)ethyl acrylate | HCID 17050 | — |
| 反応物 | 1,4-Dioxane | HCID 31275 | — |
| 反応物 | Ethyl oxoacetate | HCID 70211 | — |
| 生成物 | Diethylaminoethyl 2-(1-hydroxycarbethoxymethyl)-acrylate | HCID 86741359 | 54% |
反応手順
51 g (0.5 mole) of ethyl glyoxylate, 85.5 g (0.5 mole) of N,N-diethylaminoethyl acrylate and 5 g (62.5 millimoles) of DABCO in 100 ml of absolute dioxane are reacted by a method similar to that described in Example 6. 74 g (54% of theory) of diethylaminoethyl 2-(1-hydroxycarbethoxymethyl)-acrylate are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04652669 |
| 出典データセット | uspto-grants-1987_03 |
| ORD ID | ord-72f6b8d625a8495f9d1d729303c6e6ec |
| 出典メモ | uspto-grants-1987_03 |