化工社化工社 化学情報印刷レポート · 研究参考用
Methyl alpha-acetamidocinnamate → Acetylphenylalanine methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl alpha-acetamidocinnamate | HCID 340163 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | Acetylphenylalanine methyl ester | HCID 704002 | 82.4% |
反応手順
A second recycling of the catalyst is performed under the conditions described above, but introducing methyl α-acetamidocinnamate (1.6 g) and ethyl acetate (10 cc). Pure N-acetylphenylalanine methyl ester (1.33 g) is thus obtained with a conversion of 100%, its rotatory power being:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04654176 |
| 出典データセット | uspto-grants-1987_03 |
| ORD ID | ord-e343201433b347ff99acb0176de1801c |
| 出典メモ | uspto-grants-1987_03 |