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2-Chlorobenzyl mercaptan → Emd 39593
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Chlorobenzyl mercaptan | HCID 580759 | — |
| 反応物 | 4-chloro-1-methyl-1H-imidazo(4,5-c)pyridine | HCID 948792 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Emd 39593 | HCID 135146 | — |
反応手順
2.76 g of Na is dissolved in 180 ml of ethanol; 19.1 g of o-chlorobenzylmercaptan and 16.76 g of 4-chloro-1-methyl-1H-imidazo(4,5-c)pyridine are added; the mixture is boiled for 16 hours and evaporated; and the residue is worked up in the customary manner to give 4-o-chloro-benzylthio-1-methyl-1H-imidazo(4,5-c)pyridine of m.p. 152°-155° (from ethanol).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04654350 |
| 出典データセット | uspto-grants-1987_03 |
| ORD ID | ord-356079d3f1214307a783e51e9d01b193 |
| 出典メモ | uspto-grants-1987_03 |