Toluene → HCID 17801484、化合物

HRID 1911713ノート

反応式

HRID 1911713 の反応式
[C:1]1([CH3:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:8]1(=[O:14])[O:13][C:11](=[O:12])[CH:10]=[CH:9]1>>[C:1]1([CH3:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:11]1(=[O:12])[O:13][C:8](=[O:14])[CH:9]=[CH:10]1

参加物

3

反応物 2

HCID 1140TolueneHCID 7923Maleic Anhydride2 回

生成物 1

HCID 17801484HCID 17801484、化合物

反応条件

温度
180 °C

実験手順

125 g (1.36 moles) of toluene and 13.3 g (0.136 moles) of maleic anhydride were weighed into a 300 ml Parr reactor. The reactor was heated to 180° C. then pressurized to 60 psi with air to initiate maleic anhydride free radical formation. The solution was stirred at 180° C. for 4 hr. The reactor was cooled to room temperature, and then the contents were transferred to a round bottom flask. The toluene and maleic anhydride were removed with a rotary evaporator. Weight of residue was 1.4 g.

後処理

  1. temperatureThe reactor was cooled to room temperature
  2. customthe contents were transferred to a round bottom flask
  3. customThe toluene and maleic anhydride were removed with a rotary evaporator

出典と根拠

ORDレコード
ord-eae7501695ef4a36bb2a20400b19912f
出典データセット
uspto-grants-2013_12
特許番号
US08604110B2

反応ノート

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