Silica → N-(dipropylcarbamothioyl)-3,4,5-trimethoxybenzamide

HRID 1912241ノート

反応式

HRID 1912241 の反応式
C[CH2:2][CH2:3][CH2:4][N:5]([C:10]([NH:12][C:13]([C:15]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[C:17]([O:25][CH3:26])[CH:16]=1)=[O:14])=[S:11])[CH2:6][CH2:7][CH2:8]C.[Si](=O)=O>>[CH3:8][CH2:7][CH2:6][N:5]([C:10]([NH:12][C:13]([C:15]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[C:17]([O:25][CH3:26])[CH:16]=1)=[O:14])=[S:11])[CH2:4][CH2:3][CH3:2]

参加物

3

反応物 2

HCID 24261SilicaHCID 12357718N-(dibutylcarbamothioyl)-3,4,5-trimethoxybenzamide

生成物 1

HCID 12357717N-(dipropylcarbamothioyl)-3,4,5-trimethoxybenzamide

実験手順

A mixture of 90 parts by mass of PET obtained above and 10 parts by mass of silicon dioxide (“Silysia 445,” average particle size 2.5 μm, manufactured by Fuji Silysia Chemical Ltd.) was kneaded at 260° C. using a vented counter-rotation twin-axis extruder (L/D=35) with 30 mmφ, to prepare a PPT master (MS-4) containing 10% by mass of silicon dioxide.

後処理

  1. customwas kneaded at 260° C.

出典と根拠

ORDレコード
ord-349e197454b24492b94b51c9c718043d
出典データセット
uspto-grants-2013_12
特許番号
US08609227B2

反応ノート

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