Sulfuryl chloride → HCID 19067199、化合物

HRID 1913540ノート

反応式

HRID 1913540 の反応式
[CH3:1][CH:2]([CH3:14])[C:3]([O:5][CH:6]([O:8][C:9](SCC)=[O:10])[CH3:7])=[O:4].S(Cl)([Cl:18])(=O)=O>>[CH3:1][CH:2]([CH3:14])[C:3]([O:5][CH:6]([O:8][C:9]([Cl:18])=[O:10])[CH3:7])=[O:4]

参加物

3

反応物 2

HCID 24648Sulfuryl chlorideHCID 858856631-{[(Ethylthio)carbonyl]oxy}ethyl 2-methylpropionate

生成物 1

HCID 19067199HCID 19067199、化合物

実験手順

1-{[(Ethylthio)carbonyl]oxy}ethyl 2-methylpropionate (WO2005/66122) (412 mg) was cooled to −30° C. Sulfuryl chloride (157 μl) was added thereto, and the mixture was then stirred for 45 minutes. The solvent in the reaction solution was distilled off under reduced pressure to obtain a crude product of the title compound.

後処理

  1. distillationThe solvent in the reaction solution was distilled off under reduced pressure

出典と根拠

ORDレコード
ord-4c9388d3f6914b59bd6bf7ca6ed00553
出典データセット
uspto-grants-2013_12
特許番号
US08609710B2

反応ノート

読み込み中…