化工社化工社 化学情報印刷レポート · 研究参考用
2-Nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine → 4-(4-(3-Pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine | HCID 22041340 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-(4-(3-Pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine | HCID 22041328 | — |
反応手順
The mixture containing 2-nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine in methanol with catalytic amount of 10% Pd/C was hydrogenated until disappearance of yellow color to yield 4-(4-(3-pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine. MS: MH+=279.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08614330B2 |
| 出典データセット | uspto-grants-2013_12 |
| ORD ID | ord-8ed5c1b25eb64513822f2276de211d21 |
| 出典メモ | uspto-grants-2013_12 |