化工社化工社 化学情報印刷レポート · 研究参考用
Acrylic Acid → 2-propenoic acid, lead(2+) salt
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Lead monoxide | HCID 14827 | — |
| 生成物 | 2-propenoic acid, lead(2+) salt | HCID 10308916 | 93% |
反応手順
111.5 gms of lead monoxide is taken in 0.1 NaOH and the mixture stirred in a round bottom flask for 30 minutes at room temperature, 72 gms of acrylic acid is then adding by a dropping funnel and a period of 1 hour. The mixture is heated under reflux conditions to 35° C. for 1 hour. The yield was 93% of lead acrylate after filtration, washing and drying.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08173754B2 |
| 出典データセット | uspto-grants-2012_05 |
| ORD ID | ord-2efc357025694a09b2d39f0e11906115 |
| 出典メモ | uspto-grants-2012_05 |