化工社化工社 化学情報印刷レポート · 研究参考用
(3-Chloro-2-methylphenyl)hydrazine → 3-[2-(3-Chloro-2-methyl-phenyl)-2H-pyrazol-3-yl]-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (3-Chloro-2-methylphenyl)hydrazine | HCID 702863 | — |
| 反応物 | 3-((E)-3-Dimethylamino-acryloyl)-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one | HCID 59370123 | — |
| 生成物 | 3-[2-(3-Chloro-2-methyl-phenyl)-2H-pyrazol-3-yl]-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one | HCID 46220044 | — |
反応手順
Reaction of 3-((E)-3-dimethylamino-acryloyl)-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-6) and (3-chloro-2-methyl-phenyl)-hydrazine according to example 43 gave the desired product. MS: M=447.3 (M+H)+
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08178538B2 |
| 出典データセット | uspto-grants-2012_05 |
| ORD ID | ord-18a8e2a6feab452eb76093dab2f082e9 |
| 出典メモ | uspto-grants-2012_05 |