(2,3-Dihydro-benzo[1,4]dioxin-6-yl)-hydrazine → 3-[2-(2,3-Dihydro-benzo[1,4]dioxin-6-yl)-2H-pyrazol-3-yl]-1-(3-methoxy-phenyl)-1H-pyridazin-4-one

HRID 1924671ノート

反応式

HRID 1924671 の反応式
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([O:20][CH3:21])[CH:15]=2)[N:8]=1)=O.[O:23]1[C:28]2[CH:29]=[CH:30][C:31]([NH:33]N)=[CH:32][C:27]=2[O:26][CH2:25][CH2:24]1>>[O:23]1[C:28]2[CH:29]=[CH:30][C:31]([N:33]3[C:5]([C:7]4[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]5[CH:19]=[CH:18][CH:17]=[C:16]([O:20][CH3:21])[CH:15]=5)[N:8]=4)=[CH:4][CH:3]=[N:2]3)=[CH:32][C:27]=2[O:26][CH2:25][CH2:24]1

参加物

3

反応物 2

HCID 5164485(2,3-Dihydro-benzo[1,4]dioxin-6-yl)-hydrazineHCID 593699893-((E)-3-Dimethylamino-acryloyl)-1-(3-methoxy-phenyl)-1H-pyridazin-4-one

生成物 1

HCID 593700373-[2-(2,3-Dihydro-benzo[1,4]dioxin-6-yl)-2H-pyrazol-3-yl]-1-(3-methoxy-phenyl)-1H-pyridazin-4-one

実験手順

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(3-methoxy-phenyl)-1H-pyridazin-4-one (A-5) and (2,3-dihydro-benzo[1,4]dioxin-6-yl)-hydrazine according to the method described for example 91. MS: M=403.4 (M+H)+

後処理

  1. customThe product was obtained

出典と根拠

ORDレコード
ord-6b2b59296d9d47d796a313055778552f
出典データセット
uspto-grants-2012_05
特許番号
US08178538B2

反応ノート

読み込み中…