1,4-Dioxane hydrochloride → HCID 66879498、化合物
反応式
C(OC([N:8]1[C@H:12]([C:13]([NH2:15])=[O:14])[CH2:11][S:10][CH2:9]1)=O)(C)(C)C.[ClH:16].O1CCOCC1>>[ClH:16].[S:10]1[CH2:11][C@@H:12]([C:13]([NH2:15])=[O:14])[NH:8][CH2:9]1参加物
3
実験手順
(4R)-3-(tert-Butyloxycarbonyl)thiazolidine-4-carboxamide (8.6 g, 37.1 mmol) was dissolved in 4M HCl/dioxan (50 ml). After 1 h at room temperature the solvent was evaporated in vacuo to give a white solid identified as the title compound (6.2 g, 36.8 mmol, 99%).
後処理
- customAfter 1 h at room temperature the solvent was evaporated in vacuo
- customto give a white solid
出典と根拠
- ORDレコード
- ord-17174d8349a4427c9777b79fa6c59211
- 出典データセット
- uspto-grants-2012_05
- 特許番号
- US08183280B2
反応ノート
読み込み中…