Malonic acid, disodium salt → Zinc Malonate Dihydrate

HRID 1928694

反応式

HRID 1928694 の反応式
O.O.N[C@H](C([O-])=O)CCC([O-])=[O:8].[Zn+2:13].C([O-])(=O)CC([O-])=[O:17].[Na+].[Na+].[CH2:23]([C:27]([O-:29])=[O:28])[C:24]([O-:26])=[O:25].[Cl-].[Zn+2].[Cl-]>O>[OH2:8].[OH2:17].[C:27]([O-:29])(=[O:28])[CH2:23][C:24]([O-:26])=[O:25].[Zn+2:13]

参加物

6

反応物 4

HCID 8865Malonic acid, disodium saltHCID 9084Malonate IonHCID 3007855ZincchlorideHCID 22825209Zinc L-glutamate Dihydrate

生成物 1

HCID 86616729Zinc Malonate Dihydrate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Basically the reaction conditions found for preparation of zinc L-glutamate (Example 13) was employed. A suspension of sodium malonate (white coloured) is prepared by adding 100 mL of millipore water to 16.605 g (0.1 moles) of solid sodium malonate dibasic monohydrate (SIGMA M1875-100G, MW 166.05, CAS 26522-85-0) in a 250 mL beaker. To this suspension was added 13.628 g (0.1 moles) of solid zinc chloride (FLUKA, 96469, MW 136.3, CAS 7646-85-7). Subsequent manufacturing steps were as described in Example 13.

後処理

  1. customBasically the reaction conditions
  2. customis prepared

出典と根拠

ORDレコード
ord-0472fd44f35a4480b7a4ceff7a3e455e
出典データセット
uspto-grants-2012_05
特許番号
US08183409B2

関連ノート

読み込み中…