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4-Piperidinemethanol → [1-(Imidazole-1-sulfonyl)-piperidin-4-yl]-methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Piperidinemethanol | HCID 420771 | — |
| 反応物 | 3-(1H-Imidazol-1-ylsulfonyl)-1-methyl-1H-imidazolium trifluoromethanesulfonate | HCID 86634166 | — |
| 生成物 | [1-(Imidazole-1-sulfonyl)-piperidin-4-yl]-methanol | HCID 68915668 | — |
反応手順
[1-(Imidazole-1-sulfonyl)-piperidin-4-yl]-methanol was prepared in accordance with step A of the general method described in example 76 from 4-(hydroxymethyl)-piperidine and 3-(1H-imidazol-1-ylsulfonyl)-1-methyl-1H-imidazolium trifluoromethanesulfonate; MS: m/e=246.5 (M+H+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08183380B2 |
| 出典データセット | uspto-grants-2012_05 |
| ORD ID | ord-5d9f66db72fa42b1ae96f01e82184f4a |
| 出典メモ | uspto-grants-2012_05 |