Hexadecylamine → N-hexadecyl-N'-propylsulfamide

反応式

[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH2:18]([NH:21][S:22](Cl)(=[O:24])=[O:23])[CH2:19][CH3:20]>>[CH2:1]([NH:17][S:22]([NH:21][CH2:18][CH2:19][CH3:20])(=[O:24])=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

参加物

反応物 2

HCID 8926Hexadecylamine

HCID 13398949N-propylsulfamoyl chloride

生成物 1

HCID 16103192N-hexadecyl-N'-propylsulfamide収率 70%

実験手順

The title compound was prepared following the method described in Example 6. The starting reactants are 0.15 g (0.6 mmol) of N-hexadecylamine and 0.10 g (0.6 mmol) of N-propylsulfamoyl chloride. 0.15 g of a white solid were obtained. Yield 70%; m.p. 108-110° C.

出典と根拠

ORDレコード: ord-c55cd12b4dad476ea629dd59b73d3c04
出典データセット: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08188312B2

反応ノート

読み込み中…