Tetradecylamine → N-propyl-N'-tetradecylsulfamide

HRID 1931792ノート

反応式

[CH2:1]([NH2:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[CH2:16]([NH:19][S:20](Cl)(=[O:22])=[O:21])[CH2:17][CH3:18]>>[CH2:16]([NH:19][S:20]([NH:15][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])(=[O:22])=[O:21])[CH2:17][CH3:18]

参加物

反応物 2

HCID 16217Tetradecylamine

HCID 13398949N-propylsulfamoyl chloride

生成物 1

HCID 16103198N-propyl-N'-tetradecylsulfamide収率 55%

実験手順

The title compound was prepared following the method described Example 6. The starting reactants are 0.10 g (0.5 mmol) of N-tetradecylamine and 0.076 g (0.5 mmol) of N-propylsulfamoyl chloride. 0.092 g of a white solid are obtained. Yield 55%; m.p. 105-107° C.

出典と根拠

ORDレコード: ord-d7bfbb58b3cf4b0084d1844684b7b43c
出典データセット: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08188312B2

反応ノート

読み込み中…