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(3-Chloroprop-1-yn-1-yl)benzene → (2S,3R,6S)-2,6-Dimethyl-4-[4-(3-phenyl-prop-2-ynyloxy)-benzenesulfonyl]-morpholine-3-carboxylic acid methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (3-Chloroprop-1-yn-1-yl)benzene | HCID 287343 | — |
| 反応物 | (2S,3R,6S)-4-(4-Hydroxy-benzenesulfonyl)-2,6-dimethyl-morpholine-3-carboxylic acid methyl ester | HCID 12016690 | — |
| 生成物 | (2S,3R,6S)-2,6-Dimethyl-4-[4-(3-phenyl-prop-2-ynyloxy)-benzenesulfonyl]-morpholine-3-carboxylic acid methyl ester | HCID 12016683 | — |
反応手順
The title compound was prepared in a manner similar to the preparation in Preparation 3 from (3-chloro-prop-1-ynyl)-benzene and (2S,3R,6S)4-(4-hydroxy-benzenesulfonyl)-2,6-dimethyl-morpholine-3-carboxylic acid methyl ester. Calculated for C23H25NO6S (M+H): 444.14. Found: 444.0.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06387901B1 |
| 出典データセット | uspto-grants-2002_05 |
| ORD ID | ord-e359a953fb9d470a967ba8dd49c4bf79 |
| 出典メモ | uspto-grants-2002_05 |