Cycloheptanone → N-Cycloheptylglycine
反応式
[C:1]1(=O)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C[O:10][C:11](=[O:14])[CH2:12][NH2:13]>>[CH:1]1([NH:13][CH2:12][C:11]([OH:14])=[O:10])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1参加物
3
実験手順
N-Cycloheptylglycine was synthesized by reductive amination of cycloheptanone with glycine methyl ester following the procedure described in Gera et al., Immunopharmacology. 33:174-177 (1996). The crude product was converted to the N-Boc derivative (mp, 89-90° C.).
出典と根拠
- ORDレコード
- ord-493f57ee876946379bb0360f0d2cd6ba
- 出典データセット
- uspto-grants-2002_05
- 特許番号
- US06388054B1
反応ノート
読み込み中…