3-Cyclohexylindan-1-one → 1-Benzyl-5-(3-cyclohexylindan-1-ylidenemethyl)-1H-imidazole

HRID 1935744ノート

反応式

HRID 1935744 の反応式
[CH2:1]([N:8]1[C:12]([CH:13]=[C:14]2[C:22]3[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=3)[CH2:16][CH:15]2C2C=CC=CC=2)=[CH:11][N:10]=[CH:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:29]1(C2C3C(=CC=CC=3)C(=O)C2)[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]1>>[CH2:1]([N:8]1[C:12]([CH:13]=[C:14]2[C:22]3[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=3)[CH:16]([CH:29]3[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]3)[CH2:15]2)=[CH:11][N:10]=[CH:9]1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

参加物

3

実験手順

1-Benzyl-5-(3-cyclohexylindan-1-ylidenemethyl)-1H-imidazole was prepared as 1-benzyl-5-(2-phenylindan-1-ylidenemethyl)-1H-imidazole above except that 3-cyclo-hexylindan-1-one was used as a starting material. The crude product as its hydro-chloride salt was used in the next step without purification.

後処理

  1. customThe crude product as its hydro-chloride salt was used in the next step without purification

出典と根拠

ORDレコード
ord-fd8a84dc81fe4321b57c9398ce102bfc
出典データセット
uspto-grants-2002_05
特許番号
US06388090B2

反応ノート

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