化工社化工社 化学情報印刷レポート · 研究参考用
Triethylamine → HCID 22462540、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Triphosgene | HCID 94429 | — |
| 反応物 | 4-(Pyridin-4-yl)naphth-1-ylamine | HCID 10857012 | — |
| 反応物 | 7-(1-Methylpiperidin-4-yl)-1,2,3,5-tetrahydropyrrolo[2,3-f]indole | HCID 17898952 | — |
| 生成物 | HCID 22462540 | HCID 22462540 | — |
反応手順
The title compound was prepared in a similar manner to Example 1 from 4-(pyridin-4-yl)naphth-1-ylamine (D3, 0.16 g, 0.7 mmole), 7-(1-methylpiperidin-4-yl)-1,2,3,5-tetrahydropyrrolo[2,3-f]indole (D6, 0.15 g, 0.6 mmole), triphosgene (0.08 g, 0.28 mmole) and triethylamine (0.25 ml). This was obtained as a cream powder (0.11 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06391891B1 |
| 出典データセット | uspto-grants-2002_05 |
| ORD ID | ord-ae2ba6d2679848f7bb9b2dd18a01a4d6 |
| 出典メモ | uspto-grants-2002_05 |