化工社化工社 化学情報印刷レポート · 研究参考用
Benzyl Chloride → Benzene, [(trichlorosilyl)methyl]-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Chloride | HCID 7503 | — |
| 反応物 | Trichlorosilane | HCID 24811 | — |
| 反応物 | Benzyltributylphosphonium chloride | HCID 200231 | — |
| 生成物 | Benzene, [(trichlorosilyl)methyl]- | HCID 69863 | 802.5% |
反応手順
In the same apparatus and procedure as Example 1 above, 0.26 g (0.79 mmol) of benzyltributylphosphonium chloride, 1.00 g (7.90 mmol) of benzyl chloride, and 3.21 g (23.7 mmol) of trichlorosilane were reacted at 150° C. for 2 hrs. The resulting mixture was distilled to give 1.43 g of benzyltrichlorosilane (yield; 80%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06392077B1 |
| 出典データセット | uspto-grants-2002_05 |
| ORD ID | ord-debc401b5c524fd78cb7b8c62d241c7c |
| 出典メモ | uspto-grants-2002_05 |