化工社化工社 化学情報印刷レポート · 研究参考用
Tetrahydrofuran → CID 3084433
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tetrahydrofuran | HCID 8028 | — |
| 触媒 | 12-Wolframophosphoric acid | HCID 452313 | — |
| 生成物 | CID 3084433 | HCID 3084433 | — |
反応手順
Polymerization of THF was carried out according to the same procedure as in Example 1 except that phosphotungstic acid was used as a catalyst solution of a specific gravity of 2.05 and the reaction liquid volume V in the reactor 1 was kept constant at 420 ml. First, in order to find the relation between Mw/Mn and V/F, with P/V fixed at 1.9 kW/m3, the Mn and the Mw/Mn of PTMG obtained under conditions 1 to 3 shown in Table 1 were measured. The results obtained are shown in Table 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06395938B1 |
| 出典データセット | uspto-grants-2002_05 |
| ORD ID | ord-67e21d893bb34f52819f12c5f5be8311 |
| 出典メモ | uspto-grants-2002_05 |