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Phosphorus sulfide (P2S5) → Tetradecanethioamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| 反応物 | Tetradecanamide | HCID 69492 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | Tetradecanethioamide | HCID 21469509 | 105.6% |
反応手順
Phosphorus pentasulfide (9.8 g, 0.044 mol) was added to a mixture of tetradecanamide (8.6 g, 0.04 mol) in dry THF (250 mL) and the mixture refluxed overnight, concentrated in vacuo, and heated with methanol (200 mL), filtered, and the filtrate concentrated in vacuo to yield a pale yellow solid (10.28 g, 99%) used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05693657 |
| 出典データセット | uspto-grants-1997_12 |
| ORD ID | ord-9c1bba6281194e248ea2e149a2aa8903 |
| 出典メモ | uspto-grants-1997_12 |