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1-(4-Chlorophenyl)cyclopentanecarboxylic acid → 1-(p-Chlorophenyl)cyclopentanemethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(4-Chlorophenyl)cyclopentanecarboxylic acid | HCID 97447 | — |
| 反応物 | Aluminium lithium hydride | HCID 21226445 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | 1-(p-Chlorophenyl)cyclopentanemethanol | HCID 2724017 | — |
反応手順
This compound is prepared in a manner analogous to that of Step A of Example 4, using 2.4 grams (0.063 mole) of lithium aluminum hydride, 21.8 grams (0.097 mole) of 1-(4-chlorophenyl)-1-cyclopentanecarboxylic acid (commercially available) in about 300 mL of diethyl ether, yielding [1-(4-chlorophenyl)-1-cyclopentyl]methanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05696259 |
| 出典データセット | uspto-grants-1997_12 |
| ORD ID | ord-967488bb3a424a9a9975b2d8a3dcc24e |
| 出典メモ | uspto-grants-1997_12 |