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p-Methoxybenzophenonoxime → 1-(4-Methoxyphenyl)-1-phenylmethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-Methoxybenzophenonoxime | HCID 185567 | — |
| 反応物 | Ammonium Acetate | HCID 517165 | — |
| 反応物 | Sodium cyanoborohydride | HCID 5003444 | — |
| 触媒 | titanium(III) trichloride | HCID 10313229 | — |
| 生成物 | 1-(4-Methoxyphenyl)-1-phenylmethanamine | HCID 350041 | 76.9% |
反応手順
Following a procedure similar to that described in Preparation 12, but using 9.4 g of 4-methoxybenzophenone oxime, 33.9 g of ammonium acetate, 7.46 g of sodium cyanoborohydride, and 79 ml of a 17-19% by volume aqueous solution of titanium trichloride, 6.78 g of the title compound were obtained as an oily substance.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05698720 |
| 出典データセット | uspto-grants-1997_12 |
| ORD ID | ord-c446c783ade5406ca4deece9e630edb7 |
| 出典メモ | uspto-grants-1997_12 |