Hydrochloric Acid → HCID 67456106、化合物
反応式
[ClH:1].[N:2]1([C:8]2[N:13]=[CH:12][N:11]=[C:10]([N:14]3[C:18](=[O:19])[C:17]([N:20]4[CH:24]=[CH:23][N:22]=[N:21]4)=[CH:16][NH:15]3)[CH:9]=2)[CH2:7][CH2:6][O:5][CH2:4][CH2:3]1>O1CCOCC1>[ClH:1].[N:2]1([C:8]2[N:13]=[CH:12][N:11]=[C:10]([N:14]3[C:18](=[O:19])[C:17]([N:20]4[CH:24]=[CH:23][N:22]=[N:21]4)=[CH:16][NH:15]3)[CH:9]=2)[CH2:3][CH2:4][O:5][CH2:6][CH2:7]1参加物
4
実験手順
Batch 1: 7.5 ml of a 4 N solution of hydrogen chloride in dioxane are added to 1.7 g (5.4 mmol) of the compound from Example 71. The mixture is stirred at RT, 5 ml dioxane are added and the mixture is stirred at RT for 16 h. The solid is filtered off and washed with 5 ml dioxane. The mixture is dried under a high vacuum for 16 h, 10 ml methanol are then added and the mixture is stirred at RT for 1 h. The solid is filtered off, washed with 4 ml methanol and dried under a high vacuum. 1.6 g of the title compound are obtained.